#### Experiments

 Crystal: Space group: C 1 2 1 (No. 5) Unit cell: $$\left( \begin{array}{cccccc} 44.389 & 53.129 & 111.588 & 90.000 & 99.764 & 90.000 \end{array}\right)$$ U matrix: $$\left( \begin{array}{rrr} 0.8998 & 0.4111 & 0.1463 \\ 0.2935 & -0.8183 & 0.4943 \\ 0.3229 & -0.4018 & -0.8569 \end{array} \right)$$ B matrix: $$\left( \begin{array}{rrr} 0.0225 & 0.0000 & 0.0000 \\ 0.0000 & 0.0188 & 0.0000 \\ 0.0039 & -0.0000 & 0.0091 \end{array} \right)$$ A = UB: $$\left( \begin{array}{rrr} 0.0208 & 0.0077 & 0.0013 \\ 0.0085 & -0.0154 & 0.0045 \\ 0.0040 & -0.0076 & -0.0078 \end{array} \right)$$ A sampled at 401 scan points Average unit cell: $$\left( \begin{array}{cccccc} 44.382 & 53.103 & 111.596 & 90.000 & 99.778 & 90.000 \end{array}\right)$$

#### Experimental geometry

 Panel 1: Pixel size (mm): 0.1720, 0.1720 Image size (pixels): 2463, 2527 Trusted range: -1, 94172 Thickness (mm): 0.32 Material: Si μ: 3.21947 Fast axis: $$\left( \begin{array}{rrr} 1.0000 & 0.0034 & -0.0002 \end{array} \right)$$ Slow axis: $$\left( \begin{array}{rrr} 0.0034 & -1.0000 & 0.0011 \end{array} \right)$$ Origin: $$\left( \begin{array}{rrr} -214.2091 & 250.8724 & -324.7628 \end{array} \right)$$ Distance (mm) 324.5373 Max resolution (corners) (Å): 1.18 Max resolution (inscribed circle) (Å): 1.80 Scan: Image range: 1, 400 Oscillation: 216.00°, +0.50°/frame Goniometer: Rotation axis: $$\left( \begin{array}{rrr} 1.0000 & 0.0000 & 0.0000 \end{array} \right)$$ Fixed rotation: $$\left( \begin{array}{rrr} 1.0000 & 0.0000 & 0.0000 \\ 0.0000 & 1.0000 & 0.0000 \\ 0.0000 & 0.0000 & 1.0000 \end{array} \right)$$ Setting rotation: $$\left( \begin{array}{rrr} 1.0000 & 0.0000 & 0.0000 \\ 0.0000 & 1.0000 & 0.0000 \\ 0.0000 & 0.0000 & 1.0000 \end{array} \right)$$